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Gas law experiments generally involve pressure, volume, and temperature measurements In a few cases, other measurements such as mass and time are necessary You should remember that P, for example, is NOT a measurement; the initial and final pressure measurements are the actual measurements made in the laboratory Another common error is the application of gas law type information and calculations for non-gaseous materials Typical experiments involving these concepts are numbers 3 and 5 in the Experimental chapter A common consideration is the presence of water vapor, H2O(g) Water generates a vapor pressure, which varies with the temperature Dalton s law is used in these cases to adjust the pressure of a gas sample for the presence of water vapor The total pressure (normally atmospheric pressure) is the pressure of the gas or gases being collected and the water vapor When the pressure of an individual gas is needed, the vapor pressure of water is subtracted from the total pressure Finding the vapor pressure of water requires measuring the temperature and using a table showing vapor pressure of water versus temperature In experiments on Graham s law, time is measured The amount of time required for a sample to effuse is the measurement The amount of material effusing divided by the time elapsed is the rate of effusion Most gas law experiments use either the combined gas law or the ideal gas equation Moles of gas are a major factor in many of these experiments The combined gas law can generate the moles of a gas by adjusting the volume to STP and using Avogadro s relationship of 224 L/mol at STP The ideal gas equation gives moles from the relationship n = PV/RT Two common gas law experiments are Determination of Molar Mass by Vapor Density and Determination of the Molar Volume of a Gas While it is possible to use the combined gas law (through 224 L/mol at STP) for either of these, the ideal gas equation is easier to use The values for P, V, T, and n must be determined The temperature may be determined easily using a thermometer The temperature measurement is normally in C The C must then be converted to a Kelvin temperature (K = C + 273) Pressure is measured using a barometer If water vapor is present, a correction is needed in the pressure to compensate for its presence The vapor pressure of water is found in.

LESSONS FOR TODAY As pointed out in 7, my father exercised an extraordinary degree of power within the Packer organization Also, as

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and With these initial values of the yi and Ji, initial values of the K i can be calculated by Eq (1422) The PiSat and 4isaf values are already available from the preliminary DEW P and BUBL P calculations Equations (1419) and (1420) now provide starting values of F and dF/dV for Newton's method as represented by Eq (1421) Repeated application of this equation leads to the value of V for which Eq (1419) is satisfied for the present estimates of {Ki} remaining calculations serve to provide new estimates of {yi}and {ai] The from which to reevaluate {Ki} sequence of steps (an outer iteration) is repeated until there is This no significant change in results from one iteration to the next After the first outer iteration, the values of V and (dF/dV) used to start Newton's method (an inner iteration) are simply the

most recently calculated values Once a value of V is established, values of xi are calculated by Eq (1416) and values of yi are given by yi = Kixi Multicomponent flash calculations based on the gammdphi formulation are readily carried out by computer as outlined in Fig 145 Table 142 shows the results of a P , T-flash calculation for the system n-hexane(l)/ethanol(2)/methylcyclopentane(3)/benzene(4) This is the same system for which results of a BUBL T calculation are presented in Table 141, and the same correlations and parameter values are used here The given P and T are here 1 atm and 33415 K (61 C) The given overall mole fractions for the system { z i ) are listed in Table 142 along with the calculated values of the liquid-phase and vapor-phase mole fractions and the K-values The molar fraction of the system that is vapor is found to be V = 08166

W H AT I T TA K E S T O B E # 1

Table 142 System: n-HexanelEthanoll Methylcyclopentane(MCP)/Benzene Calculation of P,T-flash at 1 atm and 33415 K (61 C)

The pOH of a solution can also be calculated It is defined as pOH = log[OH ] The pH and the pOH are related: pH + pOH = p K w = 14 00 at 25 C

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